Sol-Gel Synthesis and Characterization of SiC Nanopowder for High-Temperature Environments

A. Abhranil *
Department of Physics, RTM Nagpur University, Nagpur, India.
Periodicity:May - August'2023

Abstract

Silicon Carbide (SiC) boasts impressive thermo-mechanical properties and exceptional resistance to high temperatures, making it a promising candidate for enhancing electric energy production efficiency. This research focuses on the sol-gel synthesis of silicon carbide (SiC) nanopowder for high-temperature environments, particularly solar receptors. The SiO2:Mg mixture, heated at 650°C for 6 hours, undergoes acid etching and subsequent washing to produce SiC. Characterization involves X-ray Powder Diffraction (XRD), Fourier-Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy (TEM). XRD confirms SiC formation, with an estimated particle size of ~30 nm. Ultrasonic velocity measurements reveal a non-linear relationship with molar concentration, suggesting strong interactions. The ultrasonic velocity increases with nanoparticle concentration but decreases with temperature due to Brownian motion. Density increases with molar concentration, indicating close packing in the nanosuspension. The study emphasizes the role of aggregation in nanocolloids and its impact on ultrasonic velocity enhancement.

Keywords

Silicon Carbide Nanosuspension, Sol-Gel Method, SiO2: Mg, SEM, TEM, Pulser Receiver, Synthesis, Characterization, High Temperatures, High Resistance.

How to Cite this Article?

Abhranil, A. (2023). Sol-Gel Synthesis and Characterization of SiC Nanopowder for High-Temperature Environments. i-manager’s Journal on Physical Sciences, 2(2), 32-37.

References

[9]. Hagen, K. D. (1999). Heat Transfer with Applications. Prentice-Hall, New Jersey, USA.
If you have access to this article please login to view the article or kindly login to purchase the article

Purchase Instant Access

Single Article

North Americas,UK,
Middle East,Europe
India Rest of world
USD EUR INR USD-ROW
Pdf 35 35 200 20
Online 35 35 200 15
Pdf & Online 35 35 400 25

Options for accessing this content:
  • If you would like institutional access to this content, please recommend the title to your librarian.
    Library Recommendation Form
  • If you already have i-manager's user account: Login above and proceed to purchase the article.
  • New Users: Please register, then proceed to purchase the article.