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Structural, Optical, Magnetic Properties of CuFe₂O₄, BaFe₂O₄Nano-Particle Synthesized via Hydrothermal Synthesis

U. Naresh*, R. Jeevan Kumar**

*_** Department of Physics, Sri Krishnadevaraya University, Anantapur, Andhra Pradesh, India.

Periodicity:October - December'2019
DOI : https://doi.org/10.26634/jms.7.3.15753

Abstract

The study of structural, optical, magnetic properties of Copper Ferrite Nanoparticles (CFN), Barium Ferrite Nanoparticles (BFN) prepared through the hydrothermal technique was carried out. The X-Ray Diffraction (XRD) pattern illustrates the formation of a single phase of face-centeredcubic structure for the CFN particles and orthorhombic structure for the BFN particles. Fourier Transform Infrared spectroscopy (FTIR) spectra revealed the confirmation of spinel form by attributing octahedral and tetrahedral bond vibrations at ν₁, ν₂ wave numbers respectively. UV–Visible spectroscopy technique was employed to determine the energy band gap. Field Emission Scanning Electron Microscopy (FESEM) and Transmission Electron Microscopy (TEM) images have shown the surface morphology as stone like particle with the agglomeration of nanoparticles, whereas Energy Dispersive X-ray spectrum (EDX) shows synthesized samples elemental evidence accurately as per the calculation. Moreover, the vibrating sample magnetometer measurements represent the particle that exhibits the super paramagnetic nature of hydrothermally synthesized copper ferrite particle.

Keywords

Hydrothermal Method, VSM, BaFe₂O₄, CuFe₂O₄, UV- Visible Spectroscopy

How to Cite this Article?

Naresh, U., and Kumar, R. J. (2019). Structural, Optical, Magnetic Properties of CuFe₂O₄, BaFe₂O₄Nano-Particle Synthesized via Hydrothermal Synthesis. i-manager’s Journal on Material Science, 7(3), 8-15. https://doi.org/10.26634/jms.7.3.15753

References

[1]. Abdellahi, M., Nejad, M. G., Saber-Samandari, S., & Khandan, A. (2017). Study of the effect of the Zn+2 content on the anisotropy and specific absorption rate of the cobalt ferrite: the application of Co1-xZnxFe₂O₄ ferrite for magnetic hyperthermia. Journal of Australian Ceramic Society, 54(2), 223-230. https://doi.org/10.1007/s41779-017-0144-5

[2]. Anjana, V., John, S., Prakash, P., Nair, A. M., Nair, A. R., Sambhudevan, S., & Shankar, B. (2018, February). Magnetic properties of copper doped nickel ferrite nanoparticles synthesized by Co precipitation method. In IOP Conference Series: Materials Science and Engineering, 310(1), 012024. https://doi.org/10.1088/17 57-899X/310/1/012024 .

[3]. Chen, Z., Wen, X., & Chen, C. (2018). Substratedependent structure, magnetic, and ferroelectric properties of Multiferroic Bi Ba FeO thin film. Journal of 0.9 0.1 3 Superconductivity and Novel Magnetism, 1-7, 2595- 2601. https://doi.org/10.1007/s10948-017-4524-4

[4]. Costa, A. F., Pimentel, P. M., Aquino, F. M., Melo, D. M. A., Melo, M. A. F., & Santos, I. M. G. (2013). Gelatin synthesis of CuFe₂O₄ and CuFeCrO₄ ceramic pigments. Materials Letters, 112, 58-61. https://doi.org/10.1016/j. matlet.2013. 08.044

[5]. Cross, W. B., Affleck, L., Kuznetsov, M. V., Parkin, I. P., & Pankhurst, Q. A. (1999). Self-propagating hightemperature synthesis of ferrites MFe₂O₄ (M= Mg, Ba, Co, Ni, Cu, Zn); reactions in an external magnetic field. Journal of Materials Chemistry, 9(10), 2545-2552. https://doi.org/10.1039/A904431K

[6]. Farid, M. T., Ahmad, I., Kanwal, M., Murtaza, G., Ali, I., Ashiq, M. N., & Khan, S. A. (2017). Magnetic and electric behavior of praseodymium substituted CuPryFe₂-yO₄ ferrites. Journal of Magnetism and Magnetic Materials, 422, 337-343. https://doi.org/10.1016/j.jmmm.2016.09. 016

[7]. Hashim, M., Raghasudha, M., Shah, J., Shirsath, S. E., Ravinder, D., Kumar, S., ... & Kotnala, R. K. (2018). High temperature dielectric studies of indium-substituted NiCuZn nanoferrites. Journal of Physics and Chemistry of Solids, 112, 29-36. https://doi.org/10.1016/j.jpcs.2017. 08.022

[8]. Kumar, N. S., Suvarna, R. P., & Naidu, K. C. B. (2019). Grain and grain boundary conduction mechanism in solgel synthesized and microwave heated Pb_0.8 - yLayCo_0.2TiO₃ (y= 0.2–0.8) nanofibers. Materials Chemistry and Physics, 223, 241-248. https://doi.org/ 10.1016/j.ceramint.2018.07.027

[9]. Kumar, N. S., Suvarna, R. P., Naidu, K. C. B., Kumar, G. R., & Ramesh, S. (2018). Structural and functional properties of sol-gel synthesized and microwave heated Pb_0.8Co_0.2 -zLazTiO₃ (z= 0.05–0.2) nanoparticles. Ceramics International, 44(16), 19408-19420. https://doi.org/10. 1016/j.ceramint.2018.07.176

[10]. Lou, Z., He, M., Wang, R., Qin, W., Zhao, D., & Chen, C. (2014). Large-scale synthesis of monodisperse magnesium ferrite via an environmentally friendly molten salt route. Inorganic Chemistry, 53(4), 2053-2057. https://doi.org/10.1021/ic402558t

[11]. Mansour, S. F., Abdo, M. A., & Kzar, F. L. (2018). Effect of Cr dopant on the structural, magnetic and dielectric properties of Cu-Zn nanoferrites. Journal of Magnetism and Magnetic Materials, 465, 176-185. https://doi.org/ 10.1016/j.jmmm.2018.05.104

[12]. Naidu, K. C. B., & Madhuri, W. (2017). Microwave processed bulk and nano NiMg ferrites: A comparative study on X-band electromagnetic interference shielding properties. Materials Chemistry and Physics, 187, 164- 176. https://doi.org/10.1016/j.matchemphys.201 6.11.062

[13]. Naidu, K. C. B., & Wuppulluri, M. (2018). Ceramic nanoparticle synthesis at lower temperatures for LTCC and MMIC Technologies. IEEE Transactions on Magnetics, 54(9), 1-8. https://doi.org/10.1109/TMAG.2018.2855663

[14]. Naresh, U., Kumar, R. J., & Naidu, K. C. B. (2019). Optical, magnetic and ferroelectric properties of Ba_0.2Cu_0.8 -xLaxFe₂O₄ (x= 0.2–0.6) nanoparticles. Ceramics International, 45(6), 7515-7523. https://doi.org/10.1016 /j.ceramint.2019.01.044

[15]. Ramaprasad, T., Kumar, R. J., Naresh, U., Prakash, M., Kothandan, D., & Naidu, K. C. B. (2018). Effect of pH value on structural and magnetic properties of CuFe₂O₄ nanoparticles synthesized by low temperature hydrothermal technique. Materials Research Express, 5 (9), 095025. https://doi.org/10.10888/2053-1591/aad860

[16]. Shinde, S. R., Kulkarni, S. D., Banpurkar, A. G., Nawathey-Dixit, R., Date, S. K., & Ogale, S. B. (2000). Magnetic properties of nanosized powders of magnetic oxides synthesized by pulsed laser ablation. Journal of Applied Physics, 88(3), 1566-1575. https://doi.org/10.1 063/1.373856

[17]. Singh, A., Singh, A., Singh, S., Tandon, P., & Yadav, R. R. (2016). Synthesis, Characterization and Gas Sensing Capability of NixCu1-xFe₂O₄ (0.0 aecurrency sign x aecurrency sign 0.8) Nanostructures Prepared via Sol-Gel Method. Journal of Inorganic and Organometallic Polymers and Materials, 26 (6), 1392-1403.https://doi.org/10.1007/s10904-016-0428-1

[18]. Vadivelan, S., & Jaya, N. V. (2016). Investigation of magnetic and structural properties of copper substituted barium ferrite powder particles via co-precipitation method. Results in Physics, 6, 843-850. https://doi.org/10. 1016/j.rinp.2016.07.013

[19]. Zhang, Y., & Stangle, G. C. (1994). Preparation of fine multicomponent oxide ceramic powder by a combustion synthesis process. Journal of Materials Research, 9(8), 1997-2004. https://doi.org/10.1557/JMR. 1994.1997

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Structural, Optical, Magnetic Properties of CuFe₂O₄, BaFe₂O₄Nano-Particle Synthesized via Hydrothermal Synthesis

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Structural, Optical, Magnetic Properties of CuFe2O4, BaFe2O4 Nano-Particle Synthesized via Hydrothermal Synthesis

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Structural, Optical, Magnetic Properties of CuFe₂O₄, BaFe₂O₄Nano-Particle Synthesized via Hydrothermal Synthesis